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LC-MS/MSによる畜水産物中のメトリブジンおよび代謝物の分析
논문 개요
| 기관명 | NDSL |
|---|---|
| 저널명 | 食品衛生學雜誌= Food Hygiene and Safety Science |
| ISSN | 0015-6426,1882-1006 |
| ISBN |
논문저자 및 소속기관 정보
| 저자(한글) | 甲斐 茂美,赤星 猛,脇 ますみ,藤 #24059,照久,金澤 秀子 |
|---|---|
| 저자(영문) | |
| 소속기관 | |
| 소속기관(영문) | |
| 출판인 | |
| 간행물 번호 | |
| 발행연도 | 2011-01-01 |
| 초록 | A method for simultaneous determination of metribuzin (MET) and three metribuzin metabolites in livestock products and seafoods by liquid chromatography-tandem mass spectrometry (LC-MS/MS) was developed. MET and its metabolites were extracted from a sample with acetonitrile, followed by InertSepC18 and BondElut SAX cartridge cleanup. The LC separation was performed on a C18 column using 0.01 mol/L ammonium formate-acetonitrile-methanol (70 :21 : 9) as the mobile phase and MS detection with both positive and negative ion electrospray ionization. The mean recoveries from 10 livestock products and seafoods were generally gt;60%, and the relative standard deviations were |
| 원문URL | http://click.ndsl.kr/servlet/OpenAPIDetailView?keyValue=03553784&target=NART&cn=NART55631084 |
| 첨부파일 |
추가정보
| 과학기술표준분류 | |
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| ICT 기술분류 | |
| DDC 분류 | |
| 주제어 (키워드) | メトリブジン,メトリブジン #33073,アミノ #20307,. メトリブジンメチルチオ基 #33073,離酸化 #20307,. メトリブジンメチルチオ基 #33073,離酸化物 #33073,アミノ #20307,. 畜産食品,水産食品,液 #20307,クロマトグラフィ #12540,/タンデム質量分析法,metribuzin,metribuzin DA,metribuzin DK,metribuzin DADK,livestock product,seafood,LC-MS/MS |