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논문 기본정보
GC/MSによる農産物中のジフェニルおよびオルトフェニルフェノ #12540;ルの分析
논문 개요
| 기관명 | NDSL |
|---|---|
| 저널명 | 食品衛生學雜誌= Food Hygiene and Safety Science |
| ISSN | 0015-6426,1882-1006 |
| ISBN |
논문저자 및 소속기관 정보
| 저자(한글) | 高橋 邦彦,堀江 正一,#24195,#28716,義文 |
|---|---|
| 저자(영문) | |
| 소속기관 | |
| 소속기관(영문) | |
| 출판인 | |
| 간행물 번호 | |
| 발행연도 | 2008-01-01 |
| 초록 | A simple determination method of diphenyl (DP) and o -phenylphenol (OPP) in agricultural products by GC/MS was examined. DP and OPP were extracted with ethyl acetate in the presence of anh. sodium sulfate. After addition of n -butanol, the extract solution was concentrated. Clean-up was achieved by shaking with graphitized bulk carbon (Supelclean ENVI-Carb). Addition of polyethylene glycol sharpened the OPP peak on GC/MS analysis.The recoveries from 9 kinds of agricultural products spiked at 0.01 and 0.5 mu;g/g each were mostly in the range of 70 to 120%, except for 50% recovery of OPP from barley spiked at 0.01 mu;g/g. The quantification limits ( S / N ge;10) of DP and OPP were 0.0013 and 0.005 mu;g/g (0.0025 and 0.01 mu;g/g in barley and soybean), respectively. |
| 원문URL | http://click.ndsl.kr/servlet/OpenAPIDetailView?keyValue=03553784&target=NART&cn=NART48717201 |
| 첨부파일 |
추가정보
| 과학기술표준분류 | |
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| ICT 기술분류 | |
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| 주제어 (키워드) | ジフェニル,オルトフェニルフェノ #12540,ル,農産物,ガスクロマトグラフィ #12540,質量分析法,ポリエチレングリコ #12540,ル,diphenyl, lt,I gt,o lt,/I gt,-phenylphenol,agricultural product,GC/MS,polyethylene glycol |