LC-MS/MSによる畜産物中のポリエ #12540;テル系抗生物質およびマクロライド系 #39366; #34411; #34220;の一 #25993;分析
기관명 | NDSL |
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저널명 | 食品衛生學雜誌= Food Hygiene and Safety Science |
ISSN | 0015-6426,1882-1006 |
ISBN |
저자(한글) | 山口 瑞香,#26623,本 健作,山口 貴弘,尾花 裕孝 |
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저자(영문) | |
소속기관 | |
소속기관(영문) | |
출판인 | |
간행물 번호 | |
발행연도 | 2011-01-01 |
초록 | A method using liquid chromatography coupled with tandem mass spectrometry (LC-MS/MS) was developed for the simultaneous determination of polyether antibiotics and macrolide anthelmintics in livestock products. The polyether antibiotics and macrolide anthelmintics were extracted from livestock products with acetonitrile and cleaned up with dispersive solid-phase extractions and a silica gel column. The quantification limits of polyether antibiotics and macrolide anthelmintics were 0.00005-0.0005 mu;g/g. Except for narasin and lasalocid in bovine liver and milk, the recoveries were 70 to 117%. The relative standard deviations met the required guideline. The developed method was applied to six kinds of livestock products. |
원문URL | http://click.ndsl.kr/servlet/OpenAPIDetailView?keyValue=03553784&target=NART&cn=NART58145728 |
첨부파일 |
과학기술표준분류 | |
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ICT 기술분류 | |
DDC 분류 | |
주제어 (키워드) | 畜産物,ポリエ #12540,テル系抗生物質,マクロライド系 #39366,#34411,#34220,. 分散固相抽出,液 #20307,クロマトグラフィ #12540,/タンデム質量分析法,livestock product,polyether antibiotic,macrolide anthelmintic,dispersive solid-phase extraction,LC-MS/MS |