農産物中ホルクロルフェニュロンのHPLC分析のための前 #20966;理法の #26908;討
기관명 | NDSL |
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저널명 | 食品衛生學雜誌= Food Hygiene and Safety Science |
ISSN | 0015-6426,1882-1006 |
ISBN |
저자(한글) | 小林 麻紀,高野 伊知 #37070,田村 康宏,富澤 早苗,立石 恭也,酒井 奈 #31298,子,上條 恭子,井部 明 #24195,永山 敏廣 |
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저자(영문) | |
소속기관 | |
소속기관(영문) | |
출판인 | |
간행물 번호 | |
발행연도 | 2007-01-01 |
초록 | A simplified method for the determination of forchlorfenuron in agricultural products by HPLC with UV detection was investigated. A chopped sample homogenate from agricultural products was extracted with acetone. The extract was filtrated and concentrated. The residues was loaded onto a Chem Elut column and extracted with ethyl acetate. The crude extract was purified on Oasis HLB and Bond Elut PSA mini-columns using a mixture of methanol and ethyl acetate. Forchlorfenuron was analyzed by HPLC with UV detection (263 nm). HPLC separation was performed on an ODS column with methanol-water as the mobile phase. Recoveries of forchlorfenuron from several agricultural products fortified at the level of 0.1 mu;g/g were in the range of 87.6-99.5%. The limit of detection ( S / N = 3) was 0.005 mu;g/g in the sample. |
원문URL | http://click.ndsl.kr/servlet/OpenAPIDetailView?keyValue=03553784&target=NART&cn=NART37167076 |
첨부파일 |
과학기술표준분류 | |
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ICT 기술분류 | |
DDC 분류 | |
주제어 (키워드) | forchlorfenuron,agricultural products,HPLC,plant growth regulator,UV detection |